Information card for entry 7125259

Structure parameters

• Formula: C28 H44 O2 P2 Pd S
• Calculated formula: C28 H44 O2 P2 Pd S
• Title of publication: Highly efficient reduction of carbon dioxide with a borane catalyzed by bis(phosphinite) pincer ligated palladium thiolate complexes.
• Authors of publication: Ma, Qiang-Qiang; Liu, Ting; Li, Shujun; Zhang, Jie; Chen, Xuenian; Guan, Hairong
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 99
• Pages of publication: 14262 - 14265
• a: 8.6167 ± 0.0009 Å
• b: 11.5992 ± 0.0012 Å
• c: 16.4263 ± 0.0017 Å
• α: 77.1791 ± 0.0012°
• β: 79.8629 ± 0.0014°
• γ: 73.9166 ± 0.0013°
• Cell volume: 1526.6 ± 0.3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0776
• Residual factor for significantly intense reflections: 0.0481
• Weighted residual factors for significantly intense reflections: 0.095
• Weighted residual factors for all reflections included in the refinement: 0.1175
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No