Information card for entry 7125551

Structure parameters

• Formula: C38 H39 Cl4 O4 Rh
• Calculated formula: C38 H39 Cl4 O4 Rh
• Title of publication: Site-selective and stepwise complexation of two M(cod)+ (M = Rh, Ir) fragments with calix[4]arene.
• Authors of publication: Ishii, Youichi; Onaka, Ken-ichi; Hirakawa, Hidehiko; Shiramizu, Kohei
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2002
• Journal issue: 10
• Pages of publication: 1150 - 1151
• a: 10.705 ± 0.004 Å
• b: 20.317 ± 0.002 Å
• c: 16.187 ± 0.002 Å
• α: 90°
• β: 93.46 ± 0.02°
• γ: 90°
• Cell volume: 3514.1 ± 1.4 ų
• Cell temperature: 294.2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.051
• Weighted residual factors for all reflections included in the refinement: 0.0513
• Goodness-of-fit parameter for all reflections included in the refinement: 1.985
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No