Information card for entry 7125552

Structure parameters

• Formula: C45 H48 Cl2 O4 Rh2
• Calculated formula: C45 H46 Cl2 O4 Rh2
• Title of publication: Site-selective and stepwise complexation of two M(cod)+ (M = Rh, Ir) fragments with calix[4]arene.
• Authors of publication: Ishii, Youichi; Onaka, Ken-ichi; Hirakawa, Hidehiko; Shiramizu, Kohei
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2002
• Journal issue: 10
• Pages of publication: 1150 - 1151
• a: 8.8 ± 0.003 Å
• b: 19.972 ± 0.003 Å
• c: 22.563 ± 0.003 Å
• α: 90°
• β: 100.86 ± 0.02°
• γ: 90°
• Cell volume: 3894.5 ± 1.6 ų
• Cell temperature: 294.2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0414
• Weighted residual factors for all reflections included in the refinement: 0.0422
• Goodness-of-fit parameter for all reflections included in the refinement: 1.422
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No