Information card for entry 7125690

Structure parameters

• Formula: C28 H24 N3 O2 P
• Calculated formula: C28 H24 N3 O2 P
• Title of publication: Cobaltaelectro-catalyzed oxidative allene annulation by electro-removable hydrazides.
• Authors of publication: Mei, Ruhuai; Fang, Xinyue; He, Liang; Sun, Junmei; Zou, Liang; Ma, Wenbo; Ackermann, Lutz
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 9
• Pages of publication: 1393 - 1396
• a: 9.7656 ± 0.0003 Å
• b: 22.5128 ± 0.0005 Å
• c: 11.5704 ± 0.0003 Å
• α: 90°
• β: 110.736 ± 0.003°
• γ: 90°
• Cell volume: 2378.98 ± 0.12 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.071
• Residual factor for significantly intense reflections: 0.0618
• Weighted residual factors for significantly intense reflections: 0.1683
• Weighted residual factors for all reflections included in the refinement: 0.1834
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No