Information card for entry 7125691

Structure parameters

• Formula: C16 H19 N O
• Calculated formula: C16 H19.009 N O
• Title of publication: Cobaltaelectro-catalyzed oxidative allene annulation by electro-removable hydrazides.
• Authors of publication: Mei, Ruhuai; Fang, Xinyue; He, Liang; Sun, Junmei; Zou, Liang; Ma, Wenbo; Ackermann, Lutz
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 9
• Pages of publication: 1393 - 1396
• a: 9.6378 ± 0.0004 Å
• b: 11.2515 ± 0.0005 Å
• c: 24.9151 ± 0.0007 Å
• α: 87.202 ± 0.003°
• β: 83.8 ± 0.003°
• γ: 78.211 ± 0.004°
• Cell volume: 2628.33 ± 0.18 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0826
• Residual factor for significantly intense reflections: 0.0746
• Weighted residual factors for significantly intense reflections: 0.2061
• Weighted residual factors for all reflections included in the refinement: 0.2191
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No