Information card for entry 7126255

Structure parameters

• Chemical name: Bis(1,2,3,4-tetrakis(isopropyl)cyclopentadienyl)-(tris(pentafluorophenyl)borylnitrido)-uranium(v) toluene sovlate
• Formula: C55.5 H62 B F15 N U
• Calculated formula: C55.5 H62 B F15 N U
• Title of publication: Lewis acid capping of a uranium(v) nitride via a uranium(iii) azide molecular square.
• Authors of publication: Boreen, Michael A.; Rao, Guodong; Villarreal, David G.; Watt, Fabian A.; Britt, R. David; Hohloch, Stephan; Arnold, John
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 33
• Pages of publication: 4535 - 4538
• a: 12.5562 ± 0.0005 Å
• b: 13.4735 ± 0.0006 Å
• c: 18.1929 ± 0.0008 Å
• α: 100.421 ± 0.002°
• β: 97.392 ± 0.002°
• γ: 116.686 ± 0.002°
• Cell volume: 2626.3 ± 0.2 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0244
• Residual factor for significantly intense reflections: 0.0218
• Weighted residual factors for significantly intense reflections: 0.0477
• Weighted residual factors for all reflections included in the refinement: 0.0488
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.7288 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No