Information card for entry 7126256

Structure parameters

• Chemical name: Bis((tris(pentafluorophenyl)borylazido)-bis(diethyl-ether)-sodium)
• Formula: C52 H40 B2 F30 N6 Na2 O4
• Calculated formula: C52 H40 B2 F30 N6 Na2 O4
• Title of publication: Lewis acid capping of a uranium(v) nitride via a uranium(iii) azide molecular square.
• Authors of publication: Boreen, Michael A.; Rao, Guodong; Villarreal, David G.; Watt, Fabian A.; Britt, R. David; Hohloch, Stephan; Arnold, John
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 33
• Pages of publication: 4535 - 4538
• a: 11.1153 ± 0.0004 Å
• b: 11.7453 ± 0.0004 Å
• c: 12.4529 ± 0.0004 Å
• α: 70.938 ± 0.001°
• β: 81.452 ± 0.001°
• γ: 72.255 ± 0.001°
• Cell volume: 1461.32 ± 0.09 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0355
• Residual factor for significantly intense reflections: 0.0331
• Weighted residual factors for significantly intense reflections: 0.0855
• Weighted residual factors for all reflections included in the refinement: 0.0877
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.7288 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No