Information card for entry 7126753

Structure parameters

• Formula: C44 H52 N6 Pd2 Si2
• Calculated formula: C44 H52 N6 Pd2 Si2
• Title of publication: Insertion of Ni(0) and Pd(0) precursors into the Si-Si bond of a disilane with two hypercoordinate silicon atoms.
• Authors of publication: Usui, Ryosuke; Sunada, Yusuke
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 60
• Pages of publication: 8464 - 8467
• a: 20.04 ± 0.03 Å
• b: 23.534 ± 0.016 Å
• c: 12.734 ± 0.017 Å
• α: 90°
• β: 126.46 ± 0.03°
• γ: 90°
• Cell volume: 4830 ± 10 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0253
• Residual factor for significantly intense reflections: 0.0211
• Weighted residual factors for significantly intense reflections: 0.0529
• Weighted residual factors for all reflections included in the refinement: 0.0544
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.4117 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No