Information card for entry 7127024

Structure parameters

• Formula: C49 H99 K3 N3 O18 Pb11 Ru
• Calculated formula: C49 H99.002 K3 N3 O18 Pb11 Ru
• Title of publication: [Cp*RuPb₁₁]^3- and [Cu@Cp*RuPb₁₁]^2-: centered and non-centered transition-metal substituted zintl icosahedra.
• Authors of publication: Li, Ai-Min; Wang, Yi; Zavalij, Peter Y.; Chen, Fu; Muñoz-Castro, Alvaro; Eichhorn, Bryan W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 74
• Pages of publication: 10859 - 10862
• a: 45.648 ± 0.005 Å
• b: 14.2377 ± 0.0016 Å
• c: 25.141 ± 0.003 Å
• α: 90°
• β: 93.2134 ± 0.0016°
• γ: 90°
• Cell volume: 16314 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0829
• Residual factor for significantly intense reflections: 0.0433
• Weighted residual factors for significantly intense reflections: 0.098
• Weighted residual factors for all reflections included in the refinement: 0.1161
• Goodness-of-fit parameter for all reflections included in the refinement: 0.946
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No