Information card for entry 7127025

Structure parameters

• Formula: C89 H150 Cu2 K4 O24 Pb22 Ru2
• Calculated formula: C89 H150 Cu2 K4 O24 Pb22 Ru2
• Title of publication: [Cp*RuPb₁₁]^3- and [Cu@Cp*RuPb₁₁]^2-: centered and non-centered transition-metal substituted zintl icosahedra.
• Authors of publication: Li, Ai-Min; Wang, Yi; Zavalij, Peter Y.; Chen, Fu; Muñoz-Castro, Alvaro; Eichhorn, Bryan W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 74
• Pages of publication: 10859 - 10862
• a: 13.18 ± 0.0009 Å
• b: 13.185 ± 0.0009 Å
• c: 20.7259 ± 0.0014 Å
• α: 92.8432 ± 0.0011°
• β: 104.274 ± 0.0011°
• γ: 102.191 ± 0.001°
• Cell volume: 3392.1 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.083
• Residual factor for significantly intense reflections: 0.0346
• Weighted residual factors for significantly intense reflections: 0.0517
• Weighted residual factors for all reflections included in the refinement: 0.0552
• Goodness-of-fit parameter for all reflections included in the refinement: 0.956
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No