Palladium(ii) catalysed cascade strategy for the synthesis of dibenzo[5,6:7,8]cycloocta[1,2-b]indol-10-ols/-10(15H)-ones: easy access to 1,3,5,7-cyclooctatetraenes (COTs).
Authors of publication
De, Sukanya; Jash, Moumita; Chowdhury, Chinmay
Journal of publication
Chemical communications (Cambridge, England)
Year of publication
2020
Journal volume
56
Journal issue
100
Pages of publication
15659 - 15662
a
17.1953 ± 0.0003 Å
b
11.2998 ± 0.0003 Å
c
23.4679 ± 0.0005 Å
α
90°
β
99.631 ± 0.001°
γ
90°
Cell volume
4495.63 ± 0.17 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 K
Number of distinct elements
5
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0399
Residual factor for significantly intense reflections
0.0394
Weighted residual factors for significantly intense reflections
0.0958
Weighted residual factors for all reflections included in the refinement
0.0962
Goodness-of-fit parameter for all reflections included in the refinement
