Palladium(ii) catalysed cascade strategy for the synthesis of dibenzo[5,6:7,8]cycloocta[1,2-b]indol-10-ols/-10(15H)-ones: easy access to 1,3,5,7-cyclooctatetraenes (COTs).
Authors of publication
De, Sukanya; Jash, Moumita; Chowdhury, Chinmay
Journal of publication
Chemical communications (Cambridge, England)
Year of publication
2020
Journal volume
56
Journal issue
100
Pages of publication
15659 - 15662
a
8.5406 ± 0.0007 Å
b
10.0271 ± 0.0008 Å
c
13.9349 ± 0.0011 Å
α
89.172 ± 0.004°
β
79.068 ± 0.004°
γ
66.547 ± 0.003°
Cell volume
1072.43 ± 0.15 Å3
Cell temperature
116 ± 2 K
Ambient diffraction temperature
116 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0745
Residual factor for significantly intense reflections
0.0713
Weighted residual factors for significantly intense reflections
0.1868
Weighted residual factors for all reflections included in the refinement
0.1905
Goodness-of-fit parameter for all reflections included in the refinement
