Palladium(ii) catalysed cascade strategy for the synthesis of dibenzo[5,6:7,8]cycloocta[1,2-b]indol-10-ols/-10(15H)-ones: easy access to 1,3,5,7-cyclooctatetraenes (COTs).
Authors of publication
De, Sukanya; Jash, Moumita; Chowdhury, Chinmay
Journal of publication
Chemical communications (Cambridge, England)
Year of publication
2020
Journal volume
56
Journal issue
100
Pages of publication
15659 - 15662
a
12.6739 ± 0.0009 Å
b
16.317 ± 0.003 Å
c
12.1213 ± 0.0013 Å
α
90°
β
109.725 ± 0.012°
γ
90°
Cell volume
2359.6 ± 0.6 Å3
Cell temperature
102 ± 2 K
Ambient diffraction temperature
102 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0506
Residual factor for significantly intense reflections
0.048
Weighted residual factors for significantly intense reflections
0.1155
Weighted residual factors for all reflections included in the refinement
0.1174
Goodness-of-fit parameter for all reflections included in the refinement
