Information card for entry 7128208

Structure parameters

• Formula: C106 H126 N4 P10 Si6 U2
• Calculated formula: C106 H126 N4 P10 Si6 U2
• Title of publication: Fragmentation, catenation, and direct functionalisation of white phosphorus by a uranium(IV)-silyl-phosphino-carbene complex.
• Authors of publication: Boronski, Josef T.; Seed, John A.; Wooles, Ashley J.; Liddle, Stephen T.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 41
• Pages of publication: 5090 - 5093
• a: 13.8687 ± 0.0002 Å
• b: 14.1074 ± 0.0003 Å
• c: 15.5642 ± 0.0002 Å
• α: 113.276 ± 0.002°
• β: 106.911 ± 0.001°
• γ: 90.138 ± 0.001°
• Cell volume: 2652.39 ± 0.09 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.025
• Residual factor for significantly intense reflections: 0.0247
• Weighted residual factors for significantly intense reflections: 0.0691
• Weighted residual factors for all reflections included in the refinement: 0.0693
• Goodness-of-fit parameter for all reflections included in the refinement: 1.113
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No