Information card for entry 7129631

Structure parameters

• Formula: C40 H47 Cl2 Mo3 O9 Sb3
• Calculated formula: C40 H47 Cl2 Mo3 O9 Sb3
• Title of publication: Synthesis of polyantimony ligand complexes starting from Cp*4Sb4
• Authors of publication: Heinl, Veronika; Balázs, Gábor; Seidl, Michael; Scheer, Manfred
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 8.537 ± 0.0002 Å
• b: 29.4147 ± 0.0005 Å
• c: 19.2872 ± 0.0003 Å
• α: 90°
• β: 100.672 ± 0.002°
• γ: 90°
• Cell volume: 4759.5 ± 0.16 ų
• Cell temperature: 123.1 ± 0.1 K
• Ambient diffraction temperature: 123.1 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0479
• Residual factor for significantly intense reflections: 0.0402
• Weighted residual factors for significantly intense reflections: 0.0956
• Weighted residual factors for all reflections included in the refinement: 0.1003
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No