Information card for entry 7129632

Structure parameters

• Formula: C76 H116 Fe4 O8 Sb4
• Calculated formula: C76 H116 Fe4 O8 Sb4
• Title of publication: Synthesis of polyantimony ligand complexes starting from Cp*4Sb4
• Authors of publication: Heinl, Veronika; Balázs, Gábor; Seidl, Michael; Scheer, Manfred
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 27.8565 ± 0.0005 Å
• b: 13.9634 ± 0.0003 Å
• c: 20.9861 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8163 ± 0.3 ų
• Cell temperature: 132 ± 13 K
• Ambient diffraction temperature: 132 ± 13 K
• Number of distinct elements: 5
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0633
• Residual factor for significantly intense reflections: 0.0538
• Weighted residual factors for significantly intense reflections: 0.1335
• Weighted residual factors for all reflections included in the refinement: 0.1425
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No