Information card for entry 7129634

Structure parameters

• Formula: C57 H32 Al Cl2 F46 O3 Sb
• Calculated formula: C56 H30 Al F46 O3 Sb
• Title of publication: Synthesis of polyantimony ligand complexes starting from Cp*4Sb4
• Authors of publication: Heinl, Veronika; Balázs, Gábor; Seidl, Michael; Scheer, Manfred
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 13.0472 ± 0.0002 Å
• b: 14.385 ± 0.0002 Å
• c: 17.8721 ± 0.0004 Å
• α: 90.162 ± 0.002°
• β: 100.136 ± 0.002°
• γ: 105.043 ± 0.001°
• Cell volume: 3184.65 ± 0.1 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0295
• Residual factor for significantly intense reflections: 0.0289
• Weighted residual factors for significantly intense reflections: 0.0754
• Weighted residual factors for all reflections included in the refinement: 0.0758
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No