Information card for entry 7129633

Structure parameters

• Formula: C62 H87 Fe4 N O8 Sb4
• Calculated formula: C62 H87 Fe4 N O8 Sb4
• Title of publication: Synthesis of polyantimony ligand complexes starting from Cp*4Sb4
• Authors of publication: Heinl, Veronika; Balázs, Gábor; Seidl, Michael; Scheer, Manfred
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 10.2505 ± 0.0002 Å
• b: 18.2944 ± 0.0005 Å
• c: 18.7216 ± 0.0004 Å
• α: 88.54 ± 0.002°
• β: 85.7954 ± 0.0018°
• γ: 75.637 ± 0.002°
• Cell volume: 3391.82 ± 0.14 ų
• Cell temperature: 123 ± 0.13 K
• Ambient diffraction temperature: 123 ± 0.13 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0456
• Residual factor for significantly intense reflections: 0.0422
• Weighted residual factors for significantly intense reflections: 0.1121
• Weighted residual factors for all reflections included in the refinement: 0.1152
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.39222 Å
• Diffraction radiation type: CuKβ
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No