Information card for entry 7129729

Structure parameters

• Formula: C132 H110 Si2
• Calculated formula: C132 H110 Si2
• Title of publication: Synthesis, properties and chemical modification of a persistent triisopropylsilylethynyl substituted tri(9-anthryl)methyl radical
• Authors of publication: Nishiuchi, Tomohiko; Ishii, Daisuke; Aibara, Seito; Sato, Hiroyasu; Kubo, Takashi
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 12.136 ± 0.001 Å
• b: 15.641 ± 0.0011 Å
• c: 16.9992 ± 0.0013 Å
• α: 70.519 ± 0.007°
• β: 69.212 ± 0.007°
• γ: 83.824 ± 0.006°
• Cell volume: 2843.8 ± 0.4 ų
• Cell temperature: 99 ± 3 K
• Ambient diffraction temperature: 99 ± 3 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2035
• Residual factor for significantly intense reflections: 0.0877
• Weighted residual factors for significantly intense reflections: 0.1929
• Weighted residual factors for all reflections included in the refinement: 0.2489
• Goodness-of-fit parameter for all reflections included in the refinement: 0.925
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No