Information card for entry 7130265

Structure parameters

• Formula: C113 H202 B2 N4 Si14
• Calculated formula: C113 H202 B2 N4 Si14
• Title of publication: Twisted push-pull disilenes obtained by direct 1,2-hydro/chloroborylation of a silylone
• Authors of publication: Koike, Taichi; Iwamoto, Takeaki
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 12.1655 ± 0.0007 Å
• b: 12.3858 ± 0.0007 Å
• c: 22.4816 ± 0.0012 Å
• α: 84.34 ± 0.001°
• β: 85.962 ± 0.001°
• γ: 61.968 ± 0.001°
• Cell volume: 2974.4 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0885
• Residual factor for significantly intense reflections: 0.0586
• Weighted residual factors for significantly intense reflections: 0.1146
• Weighted residual factors for all reflections included in the refinement: 0.1229
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No