Information card for entry 7130266

Structure parameters

• Formula: C46 H88 B Cl N2 Si7
• Calculated formula: C46 H88 B Cl N2 Si7
• Title of publication: Twisted push-pull disilenes obtained by direct 1,2-hydro/chloroborylation of a silylone
• Authors of publication: Koike, Taichi; Iwamoto, Takeaki
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 12.786 ± 0.002 Å
• b: 13.133 ± 0.002 Å
• c: 18.193 ± 0.003 Å
• α: 74.073 ± 0.004°
• β: 70.697 ± 0.004°
• γ: 66.021 ± 0.004°
• Cell volume: 2599.4 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0646
• Residual factor for significantly intense reflections: 0.0485
• Weighted residual factors for significantly intense reflections: 0.1171
• Weighted residual factors for all reflections included in the refinement: 0.128
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No