Information card for entry 7131019

Structure parameters

• Formula: C40 H57 Li N4 Ni O Si
• Calculated formula: C40 H57 Li N4 Ni O Si
• Title of publication: Synthesis and reactivity of a -1,2-dinitrogen dinickel(II) complex with C-H activated silaamidinate pincer ligand
• Authors of publication: Hu , Chaopeng; Ding, Yazhou; Bai, Yunping; Guo, Lulu; Cui, Chunming
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 11.4166 ± 0.0003 Å
• b: 12.108 ± 0.0005 Å
• c: 16.0882 ± 0.0006 Å
• α: 73.179 ± 0.003°
• β: 73.148 ± 0.003°
• γ: 67.295 ± 0.003°
• Cell volume: 1923.38 ± 0.13 ų
• Cell temperature: 293.15 K
• Ambient diffraction temperature: 293.15 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1135
• Residual factor for significantly intense reflections: 0.0701
• Weighted residual factors for significantly intense reflections: 0.1832
• Weighted residual factors for all reflections included in the refinement: 0.2131
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No