Information card for entry 7131952
| Formula |
C29 H29 Cl N4 O2 |
| Calculated formula |
C29 H29 Cl N4 O2 |
| Title of publication |
Silver-Catalyzed Pyrazole Migration and Cycloaddition Reaction of Diazo Pyrazoleamides with Ketimines |
| Authors of publication |
Shi, Maoqing; Niu, Gejun; Zhang, Tianyuan; Xu, Aimin; Zheng, Rimei; yusuf, abdulla; Shi, Taoda; Hu, Wenhao; Qian, Yu |
| Journal of publication |
Chemical Communications |
| Year of publication |
2023 |
| a |
9.9599 ± 0.0005 Å |
| b |
11.033 ± 0.0003 Å |
| c |
11.8 ± 0.0005 Å |
| α |
86.694 ± 0.003° |
| β |
71.741 ± 0.004° |
| γ |
86.666 ± 0.003° |
| Cell volume |
1228.24 ± 0.09 Å3 |
| Cell temperature |
100 ± 0.1 K |
| Ambient diffraction temperature |
100 ± 0.1 K |
| Number of distinct elements |
5 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0872 |
| Residual factor for significantly intense reflections |
0.0841 |
| Weighted residual factors for significantly intense reflections |
0.2449 |
| Weighted residual factors for all reflections included in the refinement |
0.2461 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.02 |
| Diffraction radiation probe |
x-ray |
| Diffraction radiation wavelength |
1.54184 Å |
| Diffraction radiation type |
CuKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7131952.html
