Information card for entry 7131953
| Formula |
C33 H26 N4 O2 |
| Calculated formula |
C33 H26 N4 O2 |
| Title of publication |
Silver-Catalyzed Pyrazole Migration and Cycloaddition Reaction of Diazo Pyrazoleamides with Ketimines |
| Authors of publication |
Shi, Maoqing; Niu, Gejun; Zhang, Tianyuan; Xu, Aimin; Zheng, Rimei; yusuf, abdulla; Shi, Taoda; Hu, Wenhao; Qian, Yu |
| Journal of publication |
Chemical Communications |
| Year of publication |
2023 |
| a |
13.1778 ± 0.0004 Å |
| b |
14.3635 ± 0.0004 Å |
| c |
13.5804 ± 0.0004 Å |
| α |
90° |
| β |
96.473 ± 0.003° |
| γ |
90° |
| Cell volume |
2554.1 ± 0.13 Å3 |
| Cell temperature |
99.99 ± 0.1 K |
| Ambient diffraction temperature |
99.99 ± 0.1 K |
| Number of distinct elements |
4 |
| Space group number |
14 |
| Hermann-Mauguin space group symbol |
P 1 21/n 1 |
| Hall space group symbol |
-P 2yn |
| Residual factor for all reflections |
0.0653 |
| Residual factor for significantly intense reflections |
0.0564 |
| Weighted residual factors for significantly intense reflections |
0.1546 |
| Weighted residual factors for all reflections included in the refinement |
0.1628 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.048 |
| Diffraction radiation probe |
x-ray |
| Diffraction radiation wavelength |
1.54184 Å |
| Diffraction radiation type |
CuKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7131953.html
