Information card for entry 7131954
| Formula |
C34 H28 N4 O2 |
| Calculated formula |
C34 H28 N4 O2 |
| Title of publication |
Silver-Catalyzed Pyrazole Migration and Cycloaddition Reaction of Diazo Pyrazoleamides with Ketimines |
| Authors of publication |
Shi, Maoqing; Niu, Gejun; Zhang, Tianyuan; Xu, Aimin; Zheng, Rimei; yusuf, abdulla; Shi, Taoda; Hu, Wenhao; Qian, Yu |
| Journal of publication |
Chemical Communications |
| Year of publication |
2023 |
| a |
16.8499 ± 0.0001 Å |
| b |
16.0418 ± 0.0001 Å |
| c |
19.5299 ± 0.0001 Å |
| α |
90° |
| β |
90.45 ± 0.001° |
| γ |
90° |
| Cell volume |
5278.82 ± 0.05 Å3 |
| Cell temperature |
99.99 ± 0.1 K |
| Ambient diffraction temperature |
99.99 ± 0.1 K |
| Number of distinct elements |
4 |
| Space group number |
14 |
| Hermann-Mauguin space group symbol |
P 1 21/c 1 |
| Hall space group symbol |
-P 2ybc |
| Residual factor for all reflections |
0.0412 |
| Residual factor for significantly intense reflections |
0.0404 |
| Weighted residual factors for significantly intense reflections |
0.0939 |
| Weighted residual factors for all reflections included in the refinement |
0.0943 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.146 |
| Diffraction radiation probe |
x-ray |
| Diffraction radiation wavelength |
1.54184 Å |
| Diffraction radiation type |
CuKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7131954.html
