Information card for entry 7132603

Structure parameters

• Formula: C162 H228 B9 Cl3 N18 O3 Sn3
• Calculated formula: C162 H228 B9 Cl3 N18 O3 Sn3
• Title of publication: A bromo(boryloxy) silylene and its heavier analogues.
• Authors of publication: Guthardt, Robin; Jones, Cameron
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 12
• Pages of publication: 1583 - 1586
• a: 30.8728 ± 0.0004 Å
• b: 16.2163 ± 0.0002 Å
• c: 33.9145 ± 0.0006 Å
• α: 90°
• β: 106.314 ± 0.002°
• γ: 90°
• Cell volume: 16295.4 ± 0.4 ų
• Cell temperature: 123 ± 0.1 K
• Ambient diffraction temperature: 123 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.096
• Residual factor for significantly intense reflections: 0.0477
• Weighted residual factors for significantly intense reflections: 0.112
• Weighted residual factors for all reflections included in the refinement: 0.1335
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No