Crystallography Open Database

Information card for entry 7132604

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Coordinates	7132604.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H22 N2
Calculated formula	C23 H22 N2
Title of publication	Palladium-catalyzed allylation and carbonylation: access to allylhydrazones and allyl acylhydrazones.
Authors of publication	Liang, Qianqian; Cai, Yan; Jiang, Wenjun; Pang, Mengdi; Fan, Liming; Zhang, Guoying
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	12
Pages of publication	1638 - 1641
a	10.8961 ± 0.0011 Å
b	18.4187 ± 0.0017 Å
c	9.4952 ± 0.0008 Å
α	90°
β	111.962 ± 0.005°
γ	90°
Cell volume	1767.3 ± 0.3 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	3
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1697
Residual factor for significantly intense reflections	0.0901
Weighted residual factors for significantly intense reflections	0.2066
Weighted residual factors for all reflections included in the refinement	0.2449
Goodness-of-fit parameter for all reflections included in the refinement	1.097
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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