Crystallography Open Database

Information card for entry 7132606

Preview

Coordinates	7132606.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H20 N2
Calculated formula	C22 H20 N2
Title of publication	Palladium-catalyzed allylation and carbonylation: access to allylhydrazones and allyl acylhydrazones.
Authors of publication	Liang, Qianqian; Cai, Yan; Jiang, Wenjun; Pang, Mengdi; Fan, Liming; Zhang, Guoying
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	12
Pages of publication	1638 - 1641
a	10.0309 ± 0.0009 Å
b	19.6236 ± 0.0018 Å
c	9.0074 ± 0.0008 Å
α	90°
β	104.371 ± 0.004°
γ	90°
Cell volume	1717.6 ± 0.3 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	3
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1937
Residual factor for significantly intense reflections	0.0881
Weighted residual factors for significantly intense reflections	0.1964
Weighted residual factors for all reflections included in the refinement	0.2396
Goodness-of-fit parameter for all reflections included in the refinement	1.024
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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