Crystallography Open Database

Information card for entry 7132607

Preview

Coordinates	7132607.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H20 N2 O
Calculated formula	C23 H20 N2 O
Title of publication	Palladium-catalyzed allylation and carbonylation: access to allylhydrazones and allyl acylhydrazones.
Authors of publication	Liang, Qianqian; Cai, Yan; Jiang, Wenjun; Pang, Mengdi; Fan, Liming; Zhang, Guoying
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	12
Pages of publication	1638 - 1641
a	7.4394 ± 0.0007 Å
b	10.1901 ± 0.0009 Å
c	13.5234 ± 0.0012 Å
α	98.505 ± 0.003°
β	92.733 ± 0.002°
γ	110.436 ± 0.005°
Cell volume	944.63 ± 0.15 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.113
Residual factor for significantly intense reflections	0.0731
Weighted residual factors for significantly intense reflections	0.2015
Weighted residual factors for all reflections included in the refinement	0.2311
Goodness-of-fit parameter for all reflections included in the refinement	1.078
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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