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Information card for entry 7132876
Preview
Coordinates | 7132876.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C20 H22 O5 S |
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Calculated formula | C20 H22 O5 S |
Title of publication | Dioxane promoted photochemical <i>O</i>-alkylation of 1,3-dicarbonyl compounds beyond carbene insertion into C-H and C-C bonds. |
Authors of publication | Zhou, Xinlong; Jiang, Jingjing; Zhang, Min; Wu, Qingqing; Zhu, Keyong; Shi, Dongjie; Hou, Sensen; Zhao, Jingjing; Li, Pan |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2024 |
Journal volume | 60 |
Journal issue | 32 |
Pages of publication | 4330 - 4333 |
a | 21.549 ± 0.003 Å |
b | 10.8252 ± 0.0014 Å |
c | 17.856 ± 0.003 Å |
α | 90° |
β | 113.929 ± 0.004° |
γ | 90° |
Cell volume | 3807.3 ± 1 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 4 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0624 |
Residual factor for significantly intense reflections | 0.0416 |
Weighted residual factors for significantly intense reflections | 0.0937 |
Weighted residual factors for all reflections included in the refinement | 0.1089 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.063 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7132876.html
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