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Information card for entry 7132877
Preview
Coordinates | 7132877.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C25 H22 O4 |
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Calculated formula | C25 H22 O4 |
Title of publication | Dioxane promoted photochemical <i>O</i>-alkylation of 1,3-dicarbonyl compounds beyond carbene insertion into C-H and C-C bonds. |
Authors of publication | Zhou, Xinlong; Jiang, Jingjing; Zhang, Min; Wu, Qingqing; Zhu, Keyong; Shi, Dongjie; Hou, Sensen; Zhao, Jingjing; Li, Pan |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2024 |
Journal volume | 60 |
Journal issue | 32 |
Pages of publication | 4330 - 4333 |
a | 10.2833 ± 0.0018 Å |
b | 10.038 ± 0.002 Å |
c | 20.688 ± 0.004 Å |
α | 90° |
β | 98.406 ± 0.007° |
γ | 90° |
Cell volume | 2112.6 ± 0.7 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 3 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0982 |
Residual factor for significantly intense reflections | 0.0604 |
Weighted residual factors for significantly intense reflections | 0.148 |
Weighted residual factors for all reflections included in the refinement | 0.1723 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.043 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7132877.html
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