Information card for entry 7132922

Structure parameters

• Formula: C129 H42 Ag2 Al2 As4 Cl2 F92 Mo8 O22 Sb4
• Calculated formula: C129 H42 Ag2 Al2 As4 Cl2 F92 Mo8 O22 Sb4
• Title of publication: Supramolecular compounds assembled from the heteroleptic tetrahedral complex [{CpMo(CO)₂}₂(μ,η²-AsSb)] and metal salts.
• Authors of publication: Elsayed Moussa, Mehdi; Shelyganov, Pavel A.; Seidl, Michael; Zimmermann, Lisa; Scheer, Manfred
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 35
• Pages of publication: 4703 - 4706
• a: 11.4664 ± 0.0001 Å
• b: 40.5323 ± 0.0003 Å
• c: 33.5837 ± 0.0002 Å
• α: 90°
• β: 91.704 ± 0.001°
• γ: 90°
• Cell volume: 15601.4 ± 0.2 ų
• Cell temperature: 123 ± 1 K
• Ambient diffraction temperature: 123 ± 1 K
• Number of distinct elements: 10
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0441
• Residual factor for significantly intense reflections: 0.0414
• Weighted residual factors for significantly intense reflections: 0.1114
• Weighted residual factors for all reflections included in the refinement: 0.1137
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No