Information card for entry 7132923

Structure parameters

• Formula: C108.8 H34.6 Al2 As2 Cl5.6 Cu2 F92 Mo4 N3 O14 Sb2
• Calculated formula: C107 H31 Al2 As2 Cl2 Cu2 F92 Mo4 N3 O14 Sb2
• Title of publication: Supramolecular compounds assembled from the heteroleptic tetrahedral complex [{CpMo(CO)₂}₂(μ,η²-AsSb)] and metal salts.
• Authors of publication: Elsayed Moussa, Mehdi; Shelyganov, Pavel A.; Seidl, Michael; Zimmermann, Lisa; Scheer, Manfred
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 35
• Pages of publication: 4703 - 4706
• a: 23.6343 ± 0.0003 Å
• b: 19.0078 ± 0.0002 Å
• c: 31.4538 ± 0.0003 Å
• α: 90°
• β: 98.5123 ± 0.0011°
• γ: 90°
• Cell volume: 13974.5 ± 0.3 ų
• Cell temperature: 123.01 ± 0.1 K
• Ambient diffraction temperature: 123.01 ± 0.1 K
• Number of distinct elements: 11
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0757
• Residual factor for significantly intense reflections: 0.0716
• Weighted residual factors for significantly intense reflections: 0.1842
• Weighted residual factors for all reflections included in the refinement: 0.1875
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No