Information card for entry 7133120

Structure parameters

• Formula: C47 H69 K N O2 P
• Calculated formula: C47 H69 K N O2 P
• Title of publication: A bridging bis-phosphanido-phosphinidene complex of lanthanum supported by a sterically encumbering PN ligand.
• Authors of publication: Wittwer, B.; Heim, F.; Wurst, K.; Hohloch, S.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 57
• Pages of publication: 7299 - 7302
• a: 11.463 ± 0.0004 Å
• b: 16.2623 ± 0.0005 Å
• c: 24.992 ± 0.001 Å
• α: 90°
• β: 97.374 ± 0.001°
• γ: 90°
• Cell volume: 4620.3 ± 0.3 ų
• Cell temperature: 152 K
• Ambient diffraction temperature: 152 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.049
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.1255
• Weighted residual factors for all reflections included in the refinement: 0.1303
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No