Information card for entry 7133121

Structure parameters

• Formula: C164 H216 Cl10 K2 La4 N4 O2 P4
• Calculated formula: C164 H216 Cl10 K2 La4 N4 O2 P4
• Title of publication: A Bridging Bis-Phosphanido-Phosphinidene Complex of Lanthanum Supported by a Sterically Encumbering PN Ligand
• Authors of publication: Wittwer, Benjamin; Heim, Florian; Wurst, Klaus; Hohloch, Stephan
• Journal of publication: Chemical Communications
• Year of publication: 2024
• a: 12.833 ± 0.0013 Å
• b: 16.681 ± 0.0017 Å
• c: 21.1112 ± 0.0018 Å
• α: 98.117 ± 0.003°
• β: 100.137 ± 0.003°
• γ: 108.631 ± 0.004°
• Cell volume: 4120 ± 0.7 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0664
• Residual factor for significantly intense reflections: 0.0465
• Weighted residual factors for significantly intense reflections: 0.1103
• Weighted residual factors for all reflections included in the refinement: 0.1278
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No