Information card for entry 7133160
Formula |
C27 H29 N O4 S2 |
Calculated formula |
C27 H29 N O4 S2 |
Title of publication |
Facile synthesis of 2-vinylindolines via a phosphine-mediated α-umpolung/Wittig olefination/cyclization cascade process |
Authors of publication |
Li, Shuhui; Xu, Dan; Yao, Hui; Tan, Mengting; Li, Xiaoxuan; Liu, Mingguo; Wang, Long; Huang, Nianyu; Wang, Nengzhong |
Journal of publication |
Chemical Communications |
Year of publication |
2024 |
a |
9.2418 ± 0.0001 Å |
b |
19.5215 ± 0.0003 Å |
c |
14.0366 ± 0.0002 Å |
α |
90° |
β |
99.178 ± 0.002° |
γ |
90° |
Cell volume |
2499.98 ± 0.06 Å3 |
Cell temperature |
100 ± 0.6 K |
Ambient diffraction temperature |
100 ± 0.6 K |
Number of distinct elements |
5 |
Space group number |
14 |
Hermann-Mauguin space group symbol |
P 1 21/n 1 |
Hall space group symbol |
-P 2yn |
Residual factor for all reflections |
0.0548 |
Residual factor for significantly intense reflections |
0.0453 |
Weighted residual factors for significantly intense reflections |
0.1197 |
Weighted residual factors for all reflections included in the refinement |
0.1248 |
Goodness-of-fit parameter for all reflections included in the refinement |
1.096 |
Diffraction radiation probe |
x-ray |
Diffraction radiation wavelength |
1.54184 Å |
Diffraction radiation type |
CuKα |
Has coordinates |
Yes |
Has disorder |
No |
Has Fobs |
No |
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The link is:
https://www.crystallography.net/7133160.html