Information card for entry 7133161
| Formula |
C20 H21 N O5 S |
| Calculated formula |
C20 H21 N O5 S |
| Title of publication |
Facile synthesis of 2-vinylindolines via a phosphine-mediated α-umpolung/Wittig olefination/cyclization cascade process |
| Authors of publication |
Li, Shuhui; Xu, Dan; Yao, Hui; Tan, Mengting; Li, Xiaoxuan; Liu, Mingguo; Wang, Long; Huang, Nianyu; Wang, Nengzhong |
| Journal of publication |
Chemical Communications |
| Year of publication |
2024 |
| a |
8.0093 ± 0.0009 Å |
| b |
9.9303 ± 0.001 Å |
| c |
13.0524 ± 0.0006 Å |
| α |
92.274 ± 0.006° |
| β |
107.728 ± 0.008° |
| γ |
106.033 ± 0.01° |
| Cell volume |
941.63 ± 0.17 Å3 |
| Cell temperature |
99.97 ± 0.15 K |
| Ambient diffraction temperature |
99.97 ± 0.15 K |
| Number of distinct elements |
5 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0908 |
| Residual factor for significantly intense reflections |
0.0793 |
| Weighted residual factors for significantly intense reflections |
0.2277 |
| Weighted residual factors for all reflections included in the refinement |
0.2536 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.162 |
| Diffraction radiation probe |
x-ray |
| Diffraction radiation wavelength |
1.54184 Å |
| Diffraction radiation type |
CuKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7133161.html
