Information card for entry 7133283

Structure parameters

• Formula: C24 H21 N O6 S
• Calculated formula: C24 H21 N O6 S
• Title of publication: Catalytic enantioselective [3+2] and [4+2]-annulation of cyclic <i>N</i>-sulfonyl ketimines with γ- or δ-hydroxy-α,β-unsaturated ketones.
• Authors of publication: Yang, Ji Seon; Kim, Sung-Gon
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 61
• Pages of publication: 7954 - 7957
• a: 9.792 ± 0.002 Å
• b: 10.139 ± 0.003 Å
• c: 21.399 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2124.5 ± 1 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1003
• Residual factor for significantly intense reflections: 0.0484
• Weighted residual factors for significantly intense reflections: 0.0844
• Weighted residual factors for all reflections included in the refinement: 0.0988
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No