Information card for entry 7133284

Structure parameters

• Formula: C21 H21 N O6 S
• Calculated formula: C21 H21 N O6 S
• Title of publication: Catalytic enantioselective [3+2] and [4+2]-annulation of cyclic <i>N</i>-sulfonyl ketimines with γ- or δ-hydroxy-α,β-unsaturated ketones.
• Authors of publication: Yang, Ji Seon; Kim, Sung-Gon
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 61
• Pages of publication: 7954 - 7957
• a: 8.4145 ± 0.0003 Å
• b: 8.4145 ± 0.0003 Å
• c: 56.119 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3973.4 ± 0.3 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 92
• Hermann-Mauguin space group symbol: P 41 21 2
• Hall space group symbol: P 4abw 2nw
• Residual factor for all reflections: 0.1172
• Residual factor for significantly intense reflections: 0.047
• Weighted residual factors for significantly intense reflections: 0.0918
• Weighted residual factors for all reflections included in the refinement: 0.1172
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No