Information card for entry 7133512

Structure parameters

• Formula: C34 H64 Ge N2 O5 Si4
• Calculated formula: C34 H64 Ge N2 O5 Si4
• Title of publication: Stereodivergent sila-germylenation <i>vs.</i> sila-stannylenation of an internal alkyne.
• Authors of publication: Ajithkumar, V. S.; Ghanwat, Pratiksha B.; Saha, Sougata; Pati, Swapan K.; Sen, Sakya S.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 72
• Pages of publication: 9837 - 9840
• a: 9.5714 ± 0.0009 Å
• b: 13.252 ± 0.0012 Å
• c: 17.5019 ± 0.0015 Å
• α: 97.149 ± 0.003°
• β: 97.276 ± 0.003°
• γ: 102.064 ± 0.003°
• Cell volume: 2127.2 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0357
• Residual factor for significantly intense reflections: 0.0317
• Weighted residual factors for significantly intense reflections: 0.0833
• Weighted residual factors for all reflections included in the refinement: 0.0861
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No