Information card for entry 7133513

Structure parameters

• Formula: C30 H56 N2 O4 Si4 Sn
• Calculated formula: C30 H56 N2 O4 Si4 Sn
• Title of publication: Stereodivergent sila-germylenation <i>vs.</i> sila-stannylenation of an internal alkyne.
• Authors of publication: Ajithkumar, V. S.; Ghanwat, Pratiksha B.; Saha, Sougata; Pati, Swapan K.; Sen, Sakya S.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 72
• Pages of publication: 9837 - 9840
• a: 10.2751 ± 0.001 Å
• b: 15.191 ± 0.0014 Å
• c: 25.182 ± 0.003 Å
• α: 90°
• β: 99.29 ± 0.003°
• γ: 90°
• Cell volume: 3879.1 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0354
• Residual factor for significantly intense reflections: 0.0311
• Weighted residual factors for significantly intense reflections: 0.0706
• Weighted residual factors for all reflections included in the refinement: 0.0724
• Goodness-of-fit parameter for all reflections included in the refinement: 1.151
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No