Information card for entry 7133645

Structure parameters

• Formula: C39 H71 Ge K N2 O6 Si3
• Calculated formula: C39 H71 Ge K N2 O6 Si3
• Title of publication: Metal ion-driven formation of 2<i>H</i>-silolides and -germolides.
• Authors of publication: Liu, Chenghuan; Schmidtmann, Marc; Müller, Thomas
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 80
• Pages of publication: 11295 - 11298
• a: 12.4586 ± 0.0004 Å
• b: 13.0885 ± 0.0004 Å
• c: 17.1275 ± 0.0006 Å
• α: 95.5876 ± 0.0014°
• β: 95.5032 ± 0.0014°
• γ: 115.773 ± 0.0012°
• Cell volume: 2473.14 ± 0.14 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0494
• Residual factor for significantly intense reflections: 0.0376
• Weighted residual factors for significantly intense reflections: 0.0984
• Weighted residual factors for all reflections included in the refinement: 0.1075
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No