Information card for entry 7133646

Structure parameters

• Formula: C57.67 H93 K N2 O4.66 Si4
• Calculated formula: C57.726 H93.178 K N2 O4.637 Si4
• Title of publication: Metal ion-driven formation of 2<i>H</i>-silolides and -germolides.
• Authors of publication: Liu, Chenghuan; Schmidtmann, Marc; Müller, Thomas
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 80
• Pages of publication: 11295 - 11298
• a: 10.2492 ± 0.0005 Å
• b: 13.0948 ± 0.0007 Å
• c: 23.2301 ± 0.0013 Å
• α: 103.325 ± 0.002°
• β: 91.573 ± 0.002°
• γ: 93.515 ± 0.002°
• Cell volume: 3025.3 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0737
• Residual factor for significantly intense reflections: 0.0641
• Weighted residual factors for significantly intense reflections: 0.1607
• Weighted residual factors for all reflections included in the refinement: 0.1672
• Goodness-of-fit parameter for all reflections included in the refinement: 1.122
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No