Information card for entry 7133648

Structure parameters

• Formula: C54 H87.5 K N2 O7.25 Si4
• Calculated formula: C54 H87.5 K N2 O7.25 Si4
• Title of publication: Metal ion-driven formation of 2<i>H</i>-silolides and -germolides.
• Authors of publication: Liu, Chenghuan; Schmidtmann, Marc; Müller, Thomas
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 80
• Pages of publication: 11295 - 11298
• a: 14.3502 ± 0.0006 Å
• b: 29.6584 ± 0.0012 Å
• c: 31.1403 ± 0.0012 Å
• α: 64.5446 ± 0.0016°
• β: 87.8632 ± 0.0017°
• γ: 80.4353 ± 0.0017°
• Cell volume: 11791.8 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0781
• Residual factor for significantly intense reflections: 0.0618
• Weighted residual factors for significantly intense reflections: 0.1443
• Weighted residual factors for all reflections included in the refinement: 0.1524
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No