Information card for entry 7133647

Structure parameters

• Formula: C74 H102 Cu2 N4 Si8
• Calculated formula: C74 H102 Cu2 N4 Si8
• Title of publication: Metal ion-driven formation of 2<i>H</i>-silolides and -germolides.
• Authors of publication: Liu, Chenghuan; Schmidtmann, Marc; Müller, Thomas
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 80
• Pages of publication: 11295 - 11298
• a: 14.1025 ± 0.0013 Å
• b: 17.5632 ± 0.0017 Å
• c: 15.1034 ± 0.0015 Å
• α: 90°
• β: 101.596 ± 0.003°
• γ: 90°
• Cell volume: 3664.5 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0309
• Residual factor for significantly intense reflections: 0.0253
• Weighted residual factors for significantly intense reflections: 0.068
• Weighted residual factors for all reflections included in the refinement: 0.071
• Goodness-of-fit parameter for all reflections included in the refinement: 1.003
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No