Information card for entry 7133688

Structure parameters

• Formula: C52 H82 Mg N2 O
• Calculated formula: C52 H82 Mg N2 O
• Title of publication: A series of neutral alkaline earth metal hydride complexes supported by a bulky, unsymmetrical β-diketiminate ligand, [{(^Dip/TCHPNacnac)M(μ-H)}₂] (M = Mg, Ca, Sr or Ba).
• Authors of publication: Kennedy, Dominic B.; Evans, Matthew J.; Jones, Dafydd D. L.; Parr, Joseph M.; Hill, Michael S.; Jones, Cameron
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 78
• Pages of publication: 10894 - 10897
• a: 9.7784 ± 0.0002 Å
• b: 10.7675 ± 0.0002 Å
• c: 24.1613 ± 0.0003 Å
• α: 82.949 ± 0.001°
• β: 86.01 ± 0.001°
• γ: 69.43 ± 0.002°
• Cell volume: 2362.76 ± 0.08 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0942
• Residual factor for significantly intense reflections: 0.0855
• Weighted residual factors for significantly intense reflections: 0.2355
• Weighted residual factors for all reflections included in the refinement: 0.2447
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No