Crystallography Open Database

Information card for entry 7133936

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Coordinates	7133936.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C100 H180 K4 Lu2 N10 O14
Calculated formula	C100 H180 K4 Lu2 N10 O14
Title of publication	A (C<sub>5</sub>Me<sub>5</sub>)/enolamido lutetium dinitrogen complex promoted by deprotonation on the amidinate ligand.
Authors of publication	Chen, Xiao; Xu, Hanhua; Xi, Zhenfeng; Wei, Junnian
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	87
Pages of publication	12750 - 12753
a	12.4692 ± 0.0003 Å
b	16.0421 ± 0.0004 Å
c	16.7103 ± 0.0004 Å
α	113.745 ± 0.002°
β	95.077 ± 0.002°
γ	102.135 ± 0.002°
Cell volume	2934.75 ± 0.14 Å³
Cell temperature	179.99 ± 0.1 K
Ambient diffraction temperature	179.99 ± 0.1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0372
Residual factor for significantly intense reflections	0.0282
Weighted residual factors for significantly intense reflections	0.0687
Weighted residual factors for all reflections included in the refinement	0.0727
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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