Crystallography Open Database

Information card for entry 7133937

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Coordinates	7133937.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C108 H196 K4 Lu4 N16 O12
Calculated formula	C108 H196 K4 Lu4 N16 O12
Title of publication	A (C<sub>5</sub>Me<sub>5</sub>)/enolamido lutetium dinitrogen complex promoted by deprotonation on the amidinate ligand.
Authors of publication	Chen, Xiao; Xu, Hanhua; Xi, Zhenfeng; Wei, Junnian
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	87
Pages of publication	12750 - 12753
a	49.9594 ± 0.0007 Å
b	25.6494 ± 0.0005 Å
c	20.3764 ± 0.0005 Å
α	90°
β	96.014 ± 0.002°
γ	90°
Cell volume	25967.2 ± 0.9 Å³
Cell temperature	179.99 ± 0.1 K
Ambient diffraction temperature	179.99 ± 0.1 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0695
Residual factor for significantly intense reflections	0.0465
Weighted residual factors for significantly intense reflections	0.1113
Weighted residual factors for all reflections included in the refinement	0.1197
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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