Information card for entry 7157904

Structure parameters

• Formula: C23 H18 I N O4
• Calculated formula: C23 H18 I N O4
• Title of publication: N-Alkenylation of hydroxamic acid derivatives with ethynyl benziodoxolone to synthesize cis-enamides through vinyl benziodoxolones.
• Authors of publication: Shimbo, Daisuke; Maruyama, Toshifumi; Tada, Norihiro; Itoh, Akichika
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2021
• Journal volume: 19
• Journal issue: 11
• Pages of publication: 2442 - 2447
• a: 8.9812 ± 0.0003 Å
• b: 10.2319 ± 0.0003 Å
• c: 22.2899 ± 0.0006 Å
• α: 90°
• β: 96.794 ± 0.003°
• γ: 90°
• Cell volume: 2033.94 ± 0.11 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0301
• Residual factor for significantly intense reflections: 0.0247
• Weighted residual factors for significantly intense reflections: 0.075
• Weighted residual factors for all reflections included in the refinement: 0.0783
• Goodness-of-fit parameter for all reflections included in the refinement: 1.154
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No