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Information card for entry 7157905
Preview
Coordinates | 7157905.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23 H16 |
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Calculated formula | C23 H16 |
Title of publication | Synthesis of dibenzocyclohepta[1,2-a]naphthalene derivatives from phenylacetaldehyde and alkynyl benzyl alcohols via sequential electrophilic addition and double Friedel-Crafts reactions. |
Authors of publication | Sahu, Archana K.; Unnava, Ramanjaneyulu; Behera, Bipin K.; Saikia, Anil K. |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2021 |
Journal volume | 19 |
Journal issue | 11 |
Pages of publication | 2430 - 2435 |
a | 8.7105 ± 0.0006 Å |
b | 9.787 ± 0.0007 Å |
c | 10.2324 ± 0.0012 Å |
α | 107.954 ± 0.007° |
β | 100.92 ± 0.007° |
γ | 104.829 ± 0.005° |
Cell volume | 767.28 ± 0.13 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 2 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1172 |
Residual factor for significantly intense reflections | 0.0606 |
Weighted residual factors for significantly intense reflections | 0.1672 |
Weighted residual factors for all reflections included in the refinement | 0.1977 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.031 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7157905.html
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Users of the data should acknowledge the original authors of the
structural data.